https://doi.org/10.1016/j.molliq.2019.111735, https://doi.org/10.1016/j.jct.2019.06.033, https://doi.org/10.1016/j.molliq.2018.09.076, https://doi.org/10.1016/j.jct.2014.05.009, https://doi.org/10.1016/j.snb.2012.11.097, https://doi.org/10.1016/j.fluid.2011.01.014. Citations are the number of other articles citing this article, calculated by Crossref and updated daily. 607-144-00-9 - REACH : Registration number 01-2119457561-38-0009 Adipic Acid Chemical Structure Composition. Solubilities of Adipic Acid in Cyclohexanol + Cyclohexanone Mixtures and Cyclohexanone + Cyclohexane Mixtures. Andreia de P. M. da Silva and João F. Cajaiba da Silva . Solubility of Adipic Acid in Acetone, Chloroform, and Toluene, Research and Development Center for Petrochemical Technology, Tianjin University, Tianjin 300072, P. R. China. SYNONYMS INS No. expressed as [adipic acid]water/[adipic acid]ether? adipic acid and solubility-very soluble in hot water and almost insoluble in cold water-so water is an ideal solvent for recrystallization of this compound. b. A Unified Thermodynamics Model for Solid–Liquid Equilibrium, Liquid–Liquid Equilibrium, and Vapor–Liquid Equilibrium of Cyclohexane Oxidation Systems: NRTL Model. Adipic acid is a straight-chain aliphatic dicarboxylic acid, commonly used in the manufacturing of nylon-6,6 and plasticizers. Semantic Scholar is a free, AI-powered research tool for scientific literature, based at the Allen Institute for AI. It is freely soluble in alcohol, soluble in acetone, and slightly soluble in water. Measurement and correlation for solubilities of succinic acid, glutaric acid and adipic acid in five organic solvents. The Effect of Temperature on the Solubility of 11-Cyanoundecanoic Acid in Cyclohexane, n-Hexane, and Water. The primary hazard is the threat to the environment. What is the Kd of adipic acid. Other patented processes include those using phenolas feedst… Adipic acid is found to be associated with HMG-CoA lyase deficiency, carnitine-acylcarnitine translocase deficiency, malonyl-Coa decarboxylase deficiency, and medium Chain acyl-CoA dehydrogenase deficiency, which are inborn errors of metabolism. it has a ph of 2.86 at 0.6% usage level at 25°c. FIRST-AID MEASURES Eyes Rinse with plenty of water for at least 15 minutes and seek medical attention immediately. Remember the Kd is usually the ratio of. If breathing is difficult, give oxygen. Bo Chen, Mengqi Yan, Bao Tao, Lintao Yang. Formula: C 6 H 1 0 O 4 / HOOC(CH 2) 4 COOH Molecular mass: 146.14 Boiling point: 338°C Melting point: 152°C Density: 1.36 g/cm³ Solubility in water, g/100ml at 15°C: 1.4 (moderate) ether at the same temperature. Conventionally it was manufactured from petrochemicals but in recent days it can be synthesized from renewable substrates by means of biological methods. Adipic acid (AA) CAS-No 124-04-9 . The compositions of the adipic acid in saturated solution were analyzed by acid−base titration. Also, it is less soluble in water and is soluble in alcohol and acetone. Biodegradability screening tests indicate that adipic acid is readily biodegradable. It is very soluble in water. Ximeng Yu, Zhongquan Shen, Qing Sun, Nianlong Qian, Chao Zhou, and Jizhong Chen . Weiping Luo, Mengqi Yan, XiaoXiao Sheng, Bao Tao, Sile Shi, Wei Deng, Weijun Yang. a. Current commercial adipic acid is produced from cyclohexaneby two oxidation steps. Adipic Acid occurs as white crystals or a crystalline powder. Azelaic acid is an organic compound found in wheat, rye, and barley. Solubilities of Adipic Acid and Succinic Acid in a Glutaric Acid + Acetone or n-Butanol Mixture. 355 DEFINITION Chemical names Hexanedioic acid, 1,4-Butanedicarboxylic acid Nearly all commercial adipic acid is produced from cyclohexane. PRODUCT DESCRIPTION. 3 decimal place balance. They contain carboxylic groups as their functional group.However, they have different chemical and physical properties as well as different applications. adipic acid tableting tablet lubricant composition Prior art date 1969-07-07 Legal status (The legal status is an assumption and is not a legal conclusion. Environmental: Adipic acid is not expected to volatilize from dry soil surfaces based on its extrapolated vapor pressure. Please reconnect, Authors & Adipic acid [ACD/IUPAC Name] [Wiki] Adipinsäure [German] [ACD/IUPAC Name] Asapic. RHODIACID AA - ADIPIC ACID Revision Date 28.02.2020 PRCO90076334 Version : 3.00 / GB ( EN ) 1 / 37 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1 Product identifier - Trade name RHODIACID AA - ADIPIC ACID - Index-No. Reviewers, Librarians Adipic Acid TCC’s Adipic Acid is a mildly toxic, white, crystalline compound. A sampler for determination of the temperature dependence of the solubility of solids in liquids by the isothermal method was suggested. This probably attributes to the incompatible structures. Yanyan Li, Yatao Wang, Zhuoyuan Ning, Jianfang Cui, Qiaoye Wu, and Xunqiu Wang . Dongwei Wei, Hui Li, Cheng Liu, and Baohe Wang . Will likely be mobile in the environment due to its water solubility. Weiping Luo, Mengqi Yan, Bao Tao, Sile Shi, Bo Chen. USE: Adipic acid is a commercially important chemical used during the production of nylon, plastics, lubricants, adhesives, and polyurethane foam. Determination and Correlation of Solubilities for Succinic Acid in the Adipic Acid + Glutaric Acid + Acetone Mixture and Adipic Acid in the Succinic Acid + Glutaric Acid + Acetone Mixture. An odd–even effect on solubility of dicarboxylic acids in organic solvents. Find more information about Crossref citation counts. COMPOSITION. Adipic acid is a white crystalline solid. it is used in powdered drinks, beverages, gelatin desserts, loz- … APPEARANCE. You’ve supercharged your research process with ACS and Mendeley! Please note: If you switch to a different device, you may be asked to login again with only your ACS ID. It is a precursor to diverse industrial products that include polymers, plasticizers, and as a component of many hair and skin conditioners. Adipic Acid. The solubility of adipic acid in methanol, ethanol, propanol, isopropanol, n -butanol, tert -butanol, acetone, 1,4-dioxane, acetic acid, and water was measured within the 0–60°C temperature range. Fátima L. Mota, António J. Queimada, Simão P. Pinho, Eugénia A. Macedo. Solubility of succinic acid, glutaric acid and adipic acid in propionic acid + ε-caprolactone mixtures and propionic acid + cyclohexanone mixtures: Experimental measurement and thermodynamic modeling. Clicking on the donut icon will load a page at altmetric.com with additional details about the score and the social media presence for the given article. Adipic acid is present in some plants and is a chemical in tobacco and tobacco smoke. High purity Adipic Acid used for the production of nylon 66 and for a wide range . It is used heavily in the production of textiles, particularly nylon. Marcus A. O’Mahony, Denise M. Croker, Åke C. Rasmuson, Stéphane Veesler, and Benjamin K. Hodnett . Low-cost system based on image analysis to determine solubility curves. Solubility of succinic acid, glutaric acid and adipic acid in propionic acid + ε-caprolactone + water mixtures: Experimental measurement and thermodynamic modeling. Sile Shi, Mengqi Yan, Bao Tao, Weiping Luo. Sign in to download full-size image Figure 27. Calculate the fraction of adipic acid that. Andreia de P.M. da Silva, Priscilla B. de Oliveira, Thiago B. Bandini, Amaro G. Barreto Junior, Rodrigo C. de Sena, João F. Cajaiba da Silva. Adipic acid is an aliphatic dicarboxylic acid with the formula (CH2)4 (COOH)2. Article Views are the COUNTER-compliant sum of full text article downloads since November 2008 (both PDF and HTML) across all institutions and individuals. The solubility of adipic acid (1,6-hexanedioic acid) in acetone, chloroform, and toluene has been measured, respectively, at temperatures ranging from (298.15 to 323.15) K and (298.15 to 333.15) K by a static analytical method. Its solubility is very low in water and soluble in organic solvents like alcohol and acetone. Historically, adipic acid was prepared from various fats using oxidation. the Altmetric Attention Score and how the score is calculated. Measuring the Solubility of a Quickly Transforming Metastable Polymorph of Carbamazepine. & Account Managers, For This article is cited by 151-152 °C (for adipic acid) EU Food Improvement Agents 3.2.3 Solubility Approximately 50 g/100 ml water (20 °C) This produces toxic and corrosive fumes of valeric acid and other substances. Adipic acid otherwise rarely occurs in nature, but it is known as manufactured E number food additive E355. Adipic acid is also used in baking powders instead of cream of tartar and other foods. An 84% conversion of adipic acid's carbon content to carbon dioxide was observed after 30 days aerobic incubation in soil biometer flasks at Adipic acid EC50= 31.3 mg/L 72h EC50 = 26.6 mg/L 96h Leuciscus idus: LC50 = 230 mg/L 96h EC50 = 91.9 mg/L 17 hEC50 = 85.7 mg/L 48h Persistence and DegradabilityPersistence is unlikely Bioaccumulation/ AccumulationNo information available. A sampler for determination of the temperature dependence of the solubility of solids in liquids by the isothermal method was suggested. The solubility of adipic acid in methanol, ethanol, propanol, isopropanol, n-butanol, tert-butanol, acetone, 1,4-dioxane, acetic acid, and water was measured within the 0–60°C temperature range. Find more information about Crossref citation counts. Industrial & Engineering Chemistry Research. The C6 straight-chain dicarboxylic acid is slightly soluble in water and soluble in alcohol and acetone. Cyclohexane + O2 → cyclohexanol and cyclohexanone 2. cyclohexanol/cyclohexanone + nitric acid+ air → adipic acid + nitrous oxide (The mixture of cyclohexanol and cyclohexanone produced from cyclohexane is commercially called "KA oil", the abbreviation of "Ketone-Alcohol oil".) Function: Buffer; neutralizing agent. Adipic Acid × × Purity: >99.0%(GC ... Solubility in Methanol: almost transparency: Properties (reference) Melting Point: 153 °C: Solubility in water: Slightly soluble: Degree of solubility in water : 22 g/l 20 °C: Solubility (very soluble in) Alcohol: Solubility (soluble in) Determination of the Adipic Acid Solubility Curve in Acetone by Using ATR-FTIR and Heat Flow Calorimetry. The Altmetric Attention Score is a quantitative measure of the attention that a research article has received online. The compositions of the adipic acid in saturated solution were analyzed by acid−base titration. Some features of the site may not work correctly. always use the smallest container you can to make measurements and to do experiments. It is slightly soluble in water and soluble in alcohol and acetone. Solubility prediction, solvate and cocrystal screening as tools for rational crystal engineering. 18 publications. This carboxylic acid is vital to industry. Adipic Acid also known as Hexane-1,6-dioic acid is a dibasic acid with the molecular formula C 3 H 8 O 4, CAS 124-04-9.Adipic acid is slightly soluble in water and soluble in alcohol and acetone. Solubility of drug-like molecules in pure organic solvents with the CPA EoS. It is an emulsifier for Drilling Muds and Fluids as well. Adipic Acid is an acidulant and flavoring agent. Reacts with oxidizing materials. Adipic acid (butane-1,4-dicarboxylic acid, C6 H 10 O 4) (Figure 27) is a white crystalline powder of C6-straight chain dicarboxylic acid, and is one of the most used chemicals in the world today (Table 1). The production of nylon comes from a reaction with hexamethylene diamine, also supplied by Parchem.. Adipic acid can also be found in the production of foods as a flavoring agent to add tartness.. 1. Fei Wang, Yanyan Li, Zhuoyuan Ning, Chunhua Jiang, and Xunqiu Wang . It is not hygroscopic. The solubility of adipic acid in methanol, ethanol, propanol, isopropanol, n-butanol, tert-butanol, acetone, 1,4-dioxane, acetic acid, and water was measured within the 0–60°C temperature range. Expired - Lifetime Application number Inventor George Carr Hoss White crystalline powder. Librarians & Account Managers. solubilities. use 3 decimal places. Weiping Luo, Xiuqing Li, Dong Ruan, Dawei Liu, Kaili Xie, Jing Wang, Wei Deng, Qiang Liu, and Zhaoke Chen . Mobility. These metrics are regularly updated to reflect usage leading up to the last few days. This organic compound is the most important synthetic dicarboxylic acid produced annually. It has a slight acidic taste and a very faint odor. A sampler for determination of the temperature dependence of the solubility of solids in liquids by the isothermal method was suggested. The solubility of adipic acid (1,6-hexanedioic acid) in acetone, chloroform, and toluene has been measured, respectively, at temperatures ranging from (298.15 to 323.15) K and (298.15 to 333.15) K by a static analytical method. From an industrial perspective, it is the most important dicarboxylic acid: about 2.5 billion kilograms of this white crystalline powder are produced annually, mainly as a precursor for the production of nylon. TECHNICAL DATA. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.) Inhalation Move casualty to fresh air and keep at rest. Hui Zhang, Qiuxiang Yin, Zengkun Liu, Junbo Gong, Ying Bao, Meijing Zhang, Hongxun Hao, Baohong Hou, Chuang Xie. ADI 0-5 mg/kg bw, established at the 21st JECFA in 1977. CAS Number: 124-04-9 Formula Weight: 146.14 Formula: HO 2 C(CH 2 ) 4 CO 2 H Density (g/mL): 1.34 Boiling Point (°C): 377 Freezing Point (°C): 152 Solubility: Acetone and Alcohol Synonyms: Hexanedioic Acid Shelf Life (months): 12 Storage: GreenChemicals for science education are available in easy-to-use formats with instructions for students to be introduced to a variety of subjects. Adipic acid or hexanedioic acid is the organic compound with the formula (CH2)4(COOH)2. Find more information on the Altmetric Attention Score and how the score is calculated. A modified Apelblat equation was used to correlate the experimental data. CAS: 124-04-9. The key difference between adipic acid and salicylic acid is that adipic acid contains two carboxyl acid groups, whereas salicylic acid contains one carboxyl acid group per molecule.. Adipic acid and salicylic acid are organic compounds. Measurement and Correlation for Solubilities of Adipic Acid, Glutaric Acid and Succinic Acid in Acetic Acid + Cyclohexanone Mixtures. Your Mendeley pairing has expired. If not breathing, give artificial respiration. Measurement and Correlation for Solubilities of Adipic Acid in Acetic Acid + ε-Caprolactone Mixtures and Cyclohexanone + ε-Caprolactone Mixtures. The thermodynamic parameters of solution of adipic acid in the above solvents were calculated. Malonic acid (IUPAC systematic name: propanedioic acid) is a dicarboxylic acid with structure CH 2 (COOH) 2.The ionized form of malonic acid, as well as its esters and salts, are known as malonates.For example, diethyl malonate is malonic acid's diethyl ester.The name originates from the Greek word μᾶλον (malon) meaning 'apple'. Solubilities of Adipic Acid, Glutaric Acid, and Succinic Acid in Dimethyl Glutarate + Methanol Mixtures: Experimental Measurement and Thermodynamic Modeling. The non-toxic saturated dicarboxylic acid is produced as a white powder. ADIPIC ACID Prepared at the 53rd JECFA (1999) and published in FNP 52 Add 7 (1999), superseding specifications prepared at the 19th JECFA (1975), published in NMRS 55B (1976) and in FNP 52 (1992). Solubility of succinic acid, glutaric acid and adipic acid in propionic acid + ε-caprolactone mixtures and propionic acid + cyclohexanone mixtures: Experimental measurement and thermodynamic modeling. It is a white, crystalline compound with a slight acid taste and very faint odor. You have to login with your ACS ID befor you can login with your Mendeley account. DOI: 10.1016/j.molliq.2018.09.076. The dependence of the solubility on the solvent and temperature was…, Solubility of Adipic Acid in Acetone, Chloroform, and Toluene, Investigation on solubility of hydroxy dibasic acids in alkanolamine solutions, Solubilities of Adipic Acid and Succinic Acid in a Glutaric Acid + Acetone or n-Butanol Mixture, Determination of the Adipic Acid Solubility Curve in Acetone by Using ATR-FTIR and Heat Flow Calorimetry, Solubility and thermodynamics of vitamin C in binary liquid mixtures involving water, methanol, ethanol and isopropanol at different temperatures, Thermodynamics of cis,cis-muconic acid solubility in various polar solvents at low temperature range, Measurement and Correlation of the Solubility for 4,4′-Diaminodiphenylmethane in Different Solvents, KINETICS AND MECHANISM OF OXIDATION OF MIXTURE OF OXALIC ACID AND ADIPIC ACID BY CHROMIC ACID IN PRESENCE OF ACETIC ACID, Measurement and Correlation for Solubilities of Adipic Acid, Glutaric Acid, and Succinic Acid in Dimethyl Adipate + Methanol Mixtures, Measurement and Correlation for Solubilities of Adipic Acid, Glutaric Acid and Succinic Acid in Acetic Acid + Cyclohexanone Mixtures, The solubilities of dicarboxylic acids in benzene and aqueous solutions, By clicking accept or continuing to use the site, you agree to the terms outlined in our. 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